BL2-1

Overview

Beam line 2-1 is a dedicated thin film/powder diffraction and reflectivity station. It is equipped with a Huber 2-circle goniometer and a high-resolution crystal-analyzer detector. There are several different types of sample stages to cater to a broad user-base including a motorized xyz stage, a capillary spinner, a "wet" liquid sample stage, and an Anton-Paar furnace (25-900 ºC). Data acquisition is performed using SPEC, with SPECPlot GUI interface (in-house diffractometer control, peak fitting and plotting software).

Status —

Beamline Parameters —

Energy Range Resolution ΔE/E Spot Size Flux Angular Acceptance
Focused 5500 - 17500 eV ~5 x 10-4 0.20 x 0.45 mm2 - 1.5 mrad

Optics —

Mirror Monochromator
Bent, cylindrical single crystal Si, Rh-coated Si(111) (standard configuration)

Source —

Bend Magnet

Instrumentation —

Detectors Ionization chambers, Bicron® PMT, Vortex™ Si drift detector (1 channel), Pilatus100K
Other Shutters and variable filters to alleviate beam damage. Soller slits, Si crystal analyzer

Sample Environment —

Standard Capillary spinner
Temperature control (Anton-Paar furnace): 300-1150 K
Inert gas manifold (He) for air-sensitive samples

Absorption —

584 μm Be, 10.7 m He, 15.2 μm C
Data Acquisition and Analysis


SPEAR3

Publications

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Science Highlights

Beam Line 2-1 Science Highlights

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