BL7-3

    Overview

    Beam line 7-3 is a high flux wiggler side-station optimized for x-ray absorption spectroscopy (XANES and EXAFS) in the 5.5–40 keV range, dedicated for x-ray absorption spectroscopy and EXAFS measurements on dilute biological systems. A dedicated LHe cryostat allows for routine low temperature measurements. The unfocused beam on BL7-3 is ideal for samples especially susceptible to radiation damage, such as high-valent intermediates and other oxidized species.

    The station features a double-crystal Si(220) monochromator with energy resolution up to 10-5 (ΔE/E)and small vertical entrance slits to reduce intensity glitches. Equipment includes a Canberra 30-element Ge detector for dilute samples, a passivated implanted planar silicon (PIPS) semiconductor detector for fluorescence detection, ionization chambers for transmission data, and LHe cryostats for maintaining samples at ~10 K (10-100 K default configuration, 4-200 K with LHe dewar.

    Source: 20-pole, 2-Tesla wiggler side station, 0.8 mrad acceptance

    Status

    Operational

    Beamline Parameters

    Energy Range Resolution ΔE/E Spot Size Flux
    Focused 5500-40000 eV 1 x 10-4 2 x 12 mm2 2 x 1012

    Optics

    Monochromator:
    Si(220), ϕ = 0o & 90o. double-crystal, variable-exit geometry

    Source

    Wiggler

    Instrumentation

    Detectors Canberra 30-element germanium solid state detector with Xspress3X electronics. Passivated implanted planar silicon (PIPS) semiconductor detector. Ionization chambers.
    Ancillary Soller slits and scatter guards, sample shutter to alleviate beam damage, automatic scan queueing for multiple samples/multiple spots on samples. Oxford Helium cryostat, cooled either by closed-cycle cooled He gas loop (10-100 K) or by open-cycle liquid He dewar (4-200 K)

    Sample Environment

    Standard Cryostat Sample temperature ~10 K: - Single solid sample - 4-slot solid sample cassette - Single solution sample - 5-slot solution sample cassette - Mossbauer cups

    Absorption

    762 microns Be, 205 microns C


    BL7-3

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