BL14-3b

    Overview

    Beam line 14-3a, located on the downstream table in the BL14-3 hutch, is a bending magnet side station dedicated to x-ray imaging and micro x-ray absorption spectroscopy of biological, biomedical, materials, and geological samples.  Most often used for data collection at the S K edge, BL14-3 is the only SSRL beam line capable of XAS at the P K edge. During imaging mode, a SIGRAY axially symmetric mirror system is used to achieve microfocus with a beam size of ~ 5 x 5 microns. BL14-3b is equipped with a 7-element Vortex silicon drift detector and ionization chambers for imaging. Sample positions are controlled with submicron accuracy by a Newport sample stage, inside a He environment. BL14-3b is ideal for obtaining elemental maps of small samples (about 20 microns to 25 mm) as well as performing spectroscopy on selected points in the sample (~ 5 x 5 microns).

    Status

    Operational

    Beamline Parameters

    Energy Range Resolution ΔE/E Spot Size Flux
    Focused 2100-5000 eV ~1 x 10-4 5 x 5 µm 2 x 1010 ph/sec

    Optics

    M0 Mirror M1 Mirror Monochromator Kirkpatrick-Baez System
    Flat, bent, vertically collimating, 1 m, Si, Ni-coated, Bent, toroidal, 1.2 m, Ni-coated Water-cooled Si(111) ɸ=0, Si(111) ɸ=90 double crystal
    Monochromator Crystal Glitch Library
    Microfocus

    Source

    Bend Magnet

    Instrumentation

    Detector Ionization chambers, 7-element Vortex detector, Visible CCD camera with fluorescence filters
    Sample Positioning Newport Micro sample positioner

    Sample Environment

    Helium environment
    Ambient temperature and pressure, cold stage available upon request
    Sample size: flexible, ~24 X 24 mm in one image, also accommodates larger samples.  Sample cartridges mounted on multi-position sample wheel.


    SPEAR3

    Publications

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    Science Highlights