Overview
Beam line 14-3a, located on the downstream table in the BL14-3 hutch, is a bending magnet side station dedicated to x-ray imaging and micro x-ray absorption spectroscopy of biological, biomedical, materials, and geological samples. Most often used for data collection at the S K edge, BL14-3 is the only SSRL beam line capable of XAS at the P K edge. During imaging mode, a SIGRAY axially symmetric mirror system is used to achieve microfocus with a beam size of ~ 5 x 5 microns. BL14-3b is equipped with a 7-element Vortex silicon drift detector and ionization chambers for imaging. Sample positions are controlled with submicron accuracy by a Newport sample stage, inside a He environment. BL14-3b is ideal for obtaining elemental maps of small samples (about 20 microns to 25 mm) as well as performing spectroscopy on selected points in the sample (~ 5 x 5 microns).
Status —
Beamline Parameters —
Energy Range | Resolution ΔE/E | Spot Size | Flux | |
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Focused | 2100-5000 eV | ~1 x 10-4 | 5 x 5 µm | 2 x 1010 ph/sec |
Optics —
M0 Mirror | M1 Mirror | Monochromator | Kirkpatrick-Baez System |
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Flat, bent, vertically collimating, 1 m, Si, Ni-coated, | Bent, toroidal, 1.2 m, Ni-coated | Water-cooled Si(111) ɸ=0, Si(111) ɸ=90 double crystal Monochromator Crystal Glitch Library |
Microfocus |
Source —
Instrumentation —
Detector | Ionization chambers, 7-element Vortex detector, Visible CCD camera with fluorescence filters |
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Sample Positioning | Newport Micro sample positioner |
Sample Environment —
Helium environment |
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Ambient temperature and pressure, cold stage available upon request |
Sample size: flexible, ~24 X 24 mm in one image, also accommodates larger samples. Sample cartridges mounted on multi-position sample wheel. |
