Overview
Beam line 13-3 utilizes a spherical grating monochromator (SGM) on an elliptical polarized undulator (EPU) operating in the photon energy range from 230 eV to 1700 eV with full polarization control (linear vertical/horizontal and circular left/right) covering the C, O, F K-edges, 3d transition metal L-edges, and 4f rare-earth element M-edges.
The primary experimental station at BL13-3 is optimized for Resonant Soft X-ray Scattering (RSXS). In addition, X-ray Absorption Spectroscopy (XAS) and X-ray Magnetic Circular Dichroism (XMCD) via a permanent magnet with a limited field strength (< 0.5 Tesla) can be performed using either fluorescence yield (FY) or total electron yield (TEY).
Recently, we integrated a state-of-the-art detect, so called superconducting transition-edge-sensor (TES) into the RSXS setup. It allows us to perform the resonant inelastic x-ray scattering (RIXS)/x-ray emission spectroscopy (XES) under the moderate energy resolution, 1.5 eV (FWHM) at 500 eV.
The RSXS end-station operates at UHV (< 10-9, Torr) and is equipped with a limited-angle 4-circle goniometer and a 3-axis sample positioner with temperature control from 24 K to ~320 K. Also, there are a few detectors include Schottky barrier photodiodes with the fixed pin-hole slits, a high quantum efficiency Channeltron, and a 2D-CCD detector that can be translated vertically and covers a wide area. The angular range of the detector can cover angles up to ~176° depending on the detector.
Status —
Beamline Parameters —
Energy Range | Resolution ΔE/E | Spot Size | Flux | |
---|---|---|---|---|
Focused | 270-1450 eV (XPS), 180-1450 eV (XAS) | 1 x 10-4 | 0.01 x 0.075 mm2 | 1011 - 1012 |
Optics —
M0 Mirror | Monochromator | Kirkpatrick-Baez Mirror Pair (Pt) |
---|---|---|
Horizontal flat followed by a vertical sphere, both Pt coated | Spherical Grating Monochrometer (SGM) 300 l/mm, Ni coated 600 l/mm, Ni coated 1100 l/mm, Pt coated | LN2 cooled, Si(111), ϕ = 0o , Si(311), ϕ = 0o. double-crystal. |
Source —
Instrumentation —
In-vacuum diffractometer | 4-circle goniometer (limited chi/phi angles) |
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Detectors |
|
Other | Liq-He cryostat |
UHV compatible chamber |
Sample Environment —
Sample temperature | 24 K - 320K |
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Sample size | Typically, we prefer ≤ 5 x 5 mm2sup |
Other | Magnetic field (~0.4 Tesla) through a permanent magnet (require a field cooling) |
Load-lock system (maximumly, 4 samples can be loaded) |
Publications
Publications
Highlights
Science Highlights
Beam Line 13-3 Science Highlights
Shedding New Light on the Study on High-Tc Cuprates
Unveiling the Orbital Density Waves in MnP
Quantification of Heterogeneous Degradation in Li-ion Batteries
Questioning the Universality of the Charge Density Wave Nature in Electron-doped Cuprates
Role of an Oxygen Vacancy Nanostructure on the Switchable Photovoltaic Effect in BiFeO3
Small-angle X-ray Scattering from Magnetic Clusters and Structural Grains in Magnetic Recording Media
Experimental Station 13-3
Watching Ions Hop in Superionic Nanomaterials
Panoramic Holography: Toward a Single Shot Stopwatch
Lensless MAD Imaging of Nonperiodic Nanostructures
Differential Encoding Brings Higher Resolution to X-ray Lensless Holography
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