BL13-3

    Overview

    Beam line 13-3 utilizes a spherical grating monochromator (SGM) on an elliptical polarized undulator (EPU) operating in the photon energy range from 230 eV to 1700 eV with full polarization control (linear vertical/horizontal and circular left/right) covering the C, O, F K-edges, 3d transition metal L-edges, and 4f rare-earth element M-edges.

    The primary experimental station at BL13-3 is optimized for Resonant Soft X-ray Scattering (RSXS). In addition, X-ray Absorption Spectroscopy (XAS) and X-ray Magnetic Circular Dichroism (XMCD) via a permanent magnet with a limited field strength (< 0.5 Tesla) can be performed using either fluorescence yield (FY) or total electron yield (TEY).

    Recently, we integrated a state-of-the-art detect, so called superconducting transition-edge-sensor (TES) into the RSXS setup. It allows us to perform the resonant inelastic x-ray scattering (RIXS)/x-ray emission spectroscopy (XES) under the moderate energy resolution, 1.5 eV (FWHM) at 500 eV.

    The RSXS end-station operates at UHV (< 10-9, Torr) and is equipped with a limited-angle 4-circle goniometer and a 3-axis sample positioner with temperature control from 24 K to ~320 K. Also, there are a few detectors include Schottky barrier photodiodes with the fixed pin-hole slits, a high quantum efficiency Channeltron, and a 2D-CCD detector that can be translated vertically and covers a wide area. The angular range of the detector can cover angles up to ~176° depending on the detector.

    Status

    Beamline Parameters

    Energy Range Resolution ΔE/E Spot Size Flux
    Focused 270-1450 eV (XPS), 180-1450 eV (XAS) 1 x 10-4 0.01 x 0.075 mm2 1011 - 1012

    Optics

    M0 Mirror Monochromator Kirkpatrick-Baez Mirror Pair (Pt)
    Horizontal flat followed by a vertical sphere, both Pt coated Spherical Grating Monochrometer (SGM) 300 l/mm, Ni coated 600 l/mm, Ni coated 1100 l/mm, Pt coated LN2 cooled, Si(111), ϕ = 0o , Si(311), ϕ = 0o. double-crystal.

    Source

    Undulator

    Instrumentation

    In-vacuum diffractometer 4-circle goniometer (limited chi/phi angles)
    Detectors
    • Point detector: Hamamatsu GaAsP photodiode
    • 2D detector: Greateyes in-vacuum CCD
    • Energy resolved detector: Transition-edge sensor (TES)
      • spectral coverage broader than 1 keV
      • moderate energy resolution of 1.5 eV (FWHM) at 500 eV
    Other Liq-He cryostat
    UHV compatible chamber

    Sample Environment

    Sample temperature 24 K - 320K
    Sample size Typically, we prefer ≤ 5 x 5 mm2sup
    Other Magnetic field (~0.4 Tesla) through a permanent magnet (require a field cooling)
    Load-lock system (maximumly, 4 samples can be loaded)


    BL11-3

    Publications

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