Experimental Station 2-1

Beam line 2-1 is a dedicated thin film/powder diffraction and reflectivity station. It is equipped with a Huber 2-circle goniometer and a high-resolution crystal-analyzer detector. There are several different types of sample stages to cater to a broad user-base including a motorized xyz stage, a capillary spinner, a "wet" liquid sample stage, and an Anton-Paar furnace (25-900 ºC). Data acquisition is performed using SPEC, with SPECPlot GUI interface (in-house diffractometer control, peak fitting and plotting software). 

Status
Open
Supported Techniques
Powder diffraction
Thin film diffraction
X-ray reflectivity
Main Scientific Disciplines
Environmental Sciences
Materials Sciences
Beam Line Specifications

Source

1.3 Tesla Bend Magnet, 1.5 mrad angular acceptance, side station

  Energy Range Resolution ΔE/E Spot Size Flux Angular Acceptance
Focused 5500 - 17500 eV ~5 x 10-4 0.20 x 0.45 mm2 - 1.5 mrad

 

Optics

Bent, cylindrical single crystal Si, Rh-coated

Monochromator: Si(111) (standard configuration)

Absorption

584 μm Be, 10.7 m He, 15.2 μm C

Instrumentation

Detectors: ionization chambers, Bicron® PMT, Vortex™ Si drift detector (1 channel), Pilatus100K

Other: Shutters and variable filters to alleviate beam damage. Soller slits, Si crystal analyzer  

Sample Environment

Capillary spinner

Temperature control (Anton-Paar furnace): 300-1150 K

Inert gas manifold (He) for air-sensitive samples 

Data Acquisition and Analysis

SPEC, SPECplot GUI, XMAPgui (for Vortex detector)

Beam Line Phone
650-926-5221. On-site Users: Contact the Duty Operator at 9-926-4040
Beam Line Contact

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