Beam line 11-3 is a fixed energy (12.7 keV) wiggler side-station dedicated primarily for wide angle x-ray scattering (WAXS). BL11-3 is equipped with a two-dimensional Rayonix MX225 CCD area detector. Supports sample-to-detector distances of 80-550 mm. There are sample environments available for both transmission and grazing incidence geometries. Sample heating is available for both single sample transmission and grazing incidence geometries.
Status | Open |
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Supported Techniques | X-ray diffraction X-ray scattering |
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Main Scientific Disciplines | Energy Science Environmental Sciences Materials Sciences |
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Beam Line Specifications | |||||||||||
Source24-pole, 2-Tesla wiggler, 1.0 mrad acceptance
OpticsM0 mirror: vertically focusing, flat, bent, 1 m, Si, Rh-coated Monochromator: Bent flat, side-scattering Si(311) with offcut; fixed energy at 12700 eV. Slits: Adjustable slits for defining beam to sample.
Absorption508 μm Be, 2 mm C |
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Instrumentation | Detectors: Raxyonics 225, 73.242 micron x 73.242 micron, Variable work distances 80 mm - 550 mm Vortex silicon drift detector (SSD) is available for transmission geometries. Other (available on request): Keithley 2601B source meter and Cryocon 24C temperature controller. |
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Sample Environment | GIXRD Helium Chamber: Room temperature to 350 C, Q-range 0.2 to 5 Transmission: Both single and 25 sample holder stages (1 cm aperture on sample holders) Pouch cell holder (for batteries, electrochemical fuel cells, etc.) Capillary holder |
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Data Acquisition and Analysis | SPEC, Spectre (SPEC client GUI interface), WxDiff, Igor Pro with NIKA. Hutch instrumentation computer for battery testers and other devices. |
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Beam Line Phone | 650-926-8656. On-site Users: Contact the Duty Operator at 9-650-926-4040 |
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Beam Line Contact |