Beam line 14-3a, located on the downstream table in the BL14-3 hutch, is a bending magnet side station dedicated to x-ray imaging and micro x-ray absorption spectroscopy of biological, biomedical, materials, and geological samples. Most often used for data collection at the S K edge, BL14-3 is the only SSRL beam line capable of XAS at the P K edge. During imaging mode, a Kirkpatrick-Baez (KB) mirror system is used to achieve microfocus with a beam size of ~ 5 x 5 microns. BL14-3b is equipped with a Vortex silicon drift detector and ionization chambers for imaging. Sample positions are controlled with submicron accuracy by a Newport sample stage, inside a He environment. BL14-3b is ideal for obtaining elemental maps of small samples (about 20 microns to 25 mm) as well as performing spectroscopy on selected points in the sample (~ 5 x 5 microns).
Status | Open |
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Supported Techniques | X-ray absorption spectroscopy imaging |
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Main Scientific Disciplines | Bioscience Environmental Sciences Geochemistry Materials Sciences |
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Beam Line Specifications | |||||||||||
SourceBending Magnet
OpticsM0 mirror: Flat, bent, vertically collimating, 1 m, Si, Ni-coated M1 mirror: Bent, toroidal, 1.2 m, Ni-coated Monochromator: Water-cooled Si(111) ɸ=0, Si(111) ɸ=90 double crystal Monochromator Crystal Glitch Library Crystal changes need to be scheduled and coordinated in advance with BL support staff Cynlindrical Kirkpatrick-Baez optics, Si(111) AbsorptionN/A |
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Instrumentation | Detectors: Ionization chambers, Vortex detector, 4-element Vortex detector, CCD detector, large-area PIPS Sample Positioning: Newport Micro sample positioner, 4-slot and 8-slot motorized sample holder for bulk spectroscopy |
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Sample Environment | Helium environment Ambient temperature and pressure Sample size: flexible, can measure ~24 x 24 mm in one image |
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Data Acquisition and Analysis | Microscan GUI, MicroXAS, XMap Gui, SMAK (Microtoolkit), SixPAK Useful links: Beamline information, troubleshooting, and data analysis guide UPDATED |
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Beam Line Phone | 650-926-5143. On-site Users: Contact the Duty Operator at 9-926-4040 |
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Beam Line Contact |