Overview
![BL11-3 BL11-3](/ssrl/web/sites/default/files/images/bl11-3_1.jpg)
Wide Angle X-ray Scattering 24-pole, 2-Tesla Wiggler, 1.0 mrad Acceptance Side Station
Beam line 11-3 is a fixed energy (12.7 keV) wiggler side-station dedicated primarily for wide angle x-ray scattering (WAXS). BL11-3 is equipped with a two-dimensional Rayonix MX225 CCD area detector. Supports sample-to-detector distances of 80-550 mm. There are sample environments available for both transmission and grazing incidence geometries. Sample heating is available for both single sample transmission and grazing incidence geometries.
Sample Environment —
GIXRD Helium Chamber | Room temperature to 350 C, Q-range 0.2 to 5 |
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Transmission | Both single and 25 sample holder stages (1 cm aperture on sample holders) |
Pouch cell holder (for batteries, electrochemical fuel cells, etc.) | |
Capillary holder |
Instrumentation —
Detectors | Raxyonics 225, 73.242 micron x 73.242 micron, Variable work distances 80 mm - 550 mm |
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Other | Vortex silicon drift detector (SSD) is available for transmission geometries. |
Keithley 2601B source meter and Cryocon 24C temperature controller. |
Specifications
Technical Specifications
Energy —
Energy Range | Resolution ΔE/E | Spot Size | Flux | |
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Focused | 12700 eV | ~5 x 10-4 | 3.0 x 0.15 mm | 2 x 1012 |
Optics —
M0 Mirror | Slits | Monochromator |
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Vertically focusing, flat, bent, 1 m, Si, Rh-coated | Adjustable slits for defining beam to sample. Adjustable slits for defining beam to sample. Typical beam sizes for geometries: - GIXRD (50 microns vertical x 150 microns horizontal) - Transmission (100 microns vertical x 100 microns horizontal) |
Bent flat, side-scattering Si(311) with offcut; fixed energy at 12700 eV. |
Absorption —
508 μm Be, 2 mm C |
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Publications
Publications
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Highlights
Science Highlights
Beam Line 11-3 Science Highlights
Quantification of Efficiency in Lithium Metal Negative Electrodes via Operando X-ray Diffraction
Reversible Multicolor Chromism in Layered Formamidinium Metal Halide Perovskites
Cathode Enables Quasi-Two-Stage Intercalation for Multivalent Zinc Batteries
Understanding Reaction Pathways Leading to MnO2 Polymorph Formation
Stable Solvent for Solution-based Electrical Doping of Semiconducting Polymer Films and Its Application to Organic Solar Cells
Negative-pressure Polymorphs Made by Heterostructural Alloying
Tuning the Properties in Perovskite Materials for Photovoltaics
Formation of Nanoscale Composites of Compound Semiconductors Driven by Charge Transfer
Ultra-high Charge Carrier Mobility in an Organic Semiconductor by Vertical Chain Alignment
Graphene Produces More Efficient Charge Transport Inside an Organic Semiconductor
Experimental Station 11-3
Putting the Spin on Graphite: Observing the Spins of Impurity Atoms Align
Tunable Transmittance of Near-infrared and Visible Light in Reconstructed Nanocrystal-in-Glass Composite Films
A General Relationship between Disorder, Aggregation, and Charge Transport in Conjugated Polymers
Printing Highly-aligned Single-crystalline Organic Electronic Thin Films
Crystal Structure of a Conserved Phosphatase Domain of Non-structural Protein-3 (nsp3) from the SARS Coronavirus
X-ray Characterization of Lithium-Sulfur Batteries in Action
Structure of a Thiol Monolayer-Protected Gold Nanoparticle at 1.1 Å Resolution
Effect of Chemical Pressure on the Charge Density Wave Transition in Rare-Earth Tritellurides RTe3
Ferroelectric Self-assembled PbTiO3 Perovskite Nanostructures onto (100)SrTiO3 Substrates from a Novel Microemulsion-aided Sol-Gel Preparation
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