Experimental Station 7-2

BL7-2 is dedicated to x-ray scattering and diffraction experiments in materials and environmental science. Because of high demand, research is confined to problems that can only be addressed with this unique facility. Typical programs involve intrinsically weak scattering systems, such as two-dimensional arrays and high-resolution 3-D problems.

A new Huber 6+2 -circle diffractometer is permanently installed on BL7-2 for high-resolution x-ray scattering research. The spectrometer degrees of freedom are (theta,chi,phi, mu) for the sample, and (2-theta, theta-analyzer, 2-theta-analyzer, gamma) for the detector. In addition, the input wavelength can be scanned, and the spectrometer coordinates can be remotely adjusted. Software is available for scanning between an arbitrary pair of reciprocal lattice vectors.

Status
Open
Type
X-ray
Source
20-pole, 2-Tesla Wiggler ID End Station
Energy Range

4600-16500 eV

% Time General Use
100%
Supported Techniques
Main Scientific Disciplines
Beam Line Specifications
  Energy Range Resolution ΔE/E Spot Size Flux Angular Acceptance
Focused 4600-16500 eV N/A .12 x 0.50mm N/A .4 mrad

 

Optics

Bent cylinder, single crystal Si, Rh-coated M0 mirror 
Radii: 2945 m (adjustable) x 56.1 mm 
Mean angle of incidence: 3.81 mrad 
Cut off energy: 17.7 keV 
Magnification: 1.0

Monochromator

LN2-cooled, sagitally focusing, double crystal 
Si(111) 
Upward reflecting 

Monochromator Crystal Glitch Library 

Crystal changes need to be scheduled and coordinated in advance with BL support staff.

Detector

N/A

Sample Environment

N/A

Absorption

546 micron Be, 2.4 m He, 15.2 micron C

Instrumentation

A new Huber 6+2 -circle diffractometer is permanently installed on BL7-2 for high-resolution x-ray scattering research. The spectrometer degrees of freedom are (theta,chi,phi, mu) for the sample, and (2-theta, theta-analyzer, 2-theta-analyzer, gamma) for the detector. In addition, the input wavelength can be scanned, and the spectrometer coordinates can be remotely adjusted. Software is available for scanning between an arbitrary pair of reciprocal lattice vectors.

Data Acquisition and Analysis

Diffractometer Control Software: SPEC
For questions and issues related to SPEC, contact beam line staff or send an email to

X-ray Data Booklet

Additional Notes

N/A

Beam Line Staff
Beam Line Phone
650-926-5272 . On-site Users: Contact the Duty Operator at 9-926-4040
Engineering Notes
Resource Links
Resource Documents
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