Experimental Station 2-1

BL2-1 is a dedicated powder and thin film diffraction station. It is equipped with Huber 2-circle goniometer, a high-resolution crystal-anlyzer detector, and several different types of sample stages, including a motorized xyz state, a "wet" liquid sample stage and a cryostat (temperature range 4 K - 350 K). Analysis software provided include Origin (from Microcal), GSAS (Rietveld analysis), and a searchable powder diffraction database. The main user communities are materials science, environmental science and archaeometry.

Status
Open
Type
X-ray
Source
1.3 Tesla Bend Magnet
Energy Range

4000-15800 eV

% Time General Use
100%
Supported Techniques
Main Scientific Disciplines
Beam Line Specifications
  Energy Range Resolution ΔE/E Spot Size Flux Angular Acceptance
Focused 4000-14500 eV ~5 x 10-4 .20 x 0.45mm - 1.5 mrad
Optics

Bent cylinder, single-crystal Si, Rh-coated mirror 
Radii: 2900 m (adjustable) x 52 mm 
Mean angle of incidence: 4.2 milliradians 
Cut off energy: 14.5 keV, Magnification: 1.1

Monochromator

Si(111), Si(220) Si(400), upward reflecting, double-crystal 
Monochromator Crystal Glitch Library 
Crystal changes need to be scheduled and coordinated in advance with BL support staff.

Detector

N/A

Sample Environment
Absorption

584 microns Be, 10.7 meters He, 15.2 microns C

Instrumentation

Detector: ion chambers, PMTs, current amplifiers, Soller slits, crystal analyzers.
Diffractometer: Huber 2-circle, high-resolution powder sample
LHe Cyrostat (4-350 K), hot state (25C-900C)

Data Acquisition and Analysis

Diffractometer Control Software: SPEC
For questions and issues related to SPEC, contact beam line staff or send an email to M$SPEC [at] ssrl.slac.stanford.edu
Origin 
GSAS 
X-ray Data Booklet

Additional Notes
Beam Line Staff
Beam Line Phone
650-926-5221 . On-site Users: Contact the Duty Operator at 9-926-4040
Engineering Notes
Resource Links
Resource Documents
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