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EXPERIMENTAL STATION 2-1 |
| CURRENT STATUS: | Open | ||||||||||||
| SUPPORTED TECHNIQUES: |
Powder diffraction
Thin film diffraction | ||||||||||||
| MAIN SCIENTIFIC DISCIPLINES: | Materials / Environmental | ||||||||||||
| % TIME GENERAL USE: | 100% | ||||||||||||
| SCHEDULING: | Proposal Submittal and Scheduling Procedures Current SPEAR and Beam Line Schedules |
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| SOURCE: | 1.3 Tesla Bend Magnet | ||||||||||||
BEAM LINE SPECIFICATIONS:
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| OPTICS: |
Bent cylinder, single-crystal Si, Rh-coated mirror
Radii: 2900 m (adjustable) x 52 mm Mean angle of incidence: 4.2 milliradians Cut off energy: 14.5 keV, Magnification: 1.1 |
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| MONOCHROMATOR: | Si(111), Si(220) Si(400), upward
reflecting, double-crystal
Monochromator Crystal Glitch Library Crystal changes need to be scheduled and coordinated in advance with BL support staff. |
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| ABSORPTION: | 584 microns Be, 10.7 meters He, 15.2 microns C | ||||||||||||
| INSTRUMENTATION: |
Detector: ion chambers, PMTs,
current amplifiers, Soller slits, crystal analyzers.
Diffractometer: Huber 2-circle, high-resolution powder sample LHe Cyrostat (4-350 K), hot state (25C-900C) |
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| DATA ACQUISITION AND ANALYSIS: | Diffractometer Control Software: SPEC For questions and issues related to SPEC, contact beam line staff or send an email to M$SPEC@ssrl.slac.stanford.edu Origin GSAS X-ray Data Booklet |
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| RESPONSIBLE STAFF: | Beam Line Technical Support: Charles Troxel, 650-714-7821
Scientific Support: Apurva Mehta, Stefan Mannsfeld, Mike Toney, 650-926-2056 |
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| BEAM LINE PHONE NUMBER: | 650-926-5221 On-site Users: Contact the Duty Operator at 9-926-4040 | ||||||||||||
| GENERAL DESCRIPTION: | BL2-1 is a dedicated powder and thin film diffraction station. It is equipped with Huber 2-circle goniometer, a high-resolution crystal-anlyzer detector, and several different types of sample stages, including a motorized xyz state, a "wet" liquid sample stage and a cryostat (temperature range 4 K - 350 K). Analysis software provided include Origin (from Microcal), GSAS (Rietveld analysis), and a searchable powder diffraction database. The main user communities are materials science, environmental science and archaeometry. | ||||||||||||
| Sample Preparation Labs: | The SSRL Structural Molecular Biology (SMB) Sample Preparation Laboratories are available to users by prearrangement. To use a laboratory, users must complete laboratory training, and provide a list of all chemicals to be brought, used or stored in the Sample Preparation Laboratory. For details, contact Cynthia Patty (650-926-3925). | ||||||||||||
| SCIENTIFIC APPLICATIONS /
SELECTED RESULTS: |
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| ENGINEERING NOTES | http://www-ssrl.slac.stanford.edu/safety/beamlines/bl2/ | ||||||||||||
| SSRL | Beamlines | User Admin | Safety |
| Last Updated: | 27 JAN 2011 |
| Content Owner: | Bart Johnson |
| Page Editor: | Lisa Dunn |